2,2-Dimethylhexane → 2-Methylbuta-1,3-diene--2-methylprop-1-ene (1/1)

HRID 236382

반응식

HRID 236382 반응식
[CH3:1][C:2](C)([CH3:7])[CH2:3][CH2:4]CC>C(Cl)(Cl)(Cl)Cl>[CH3:3][C:2]([CH3:7])=[CH2:1].[CH3:7][C:2]([CH:3]=[CH2:4])=[CH2:1]

참가 물질

3

반응물 1

HCID 115512,2-Dimethylhexane

생성물 1

HCID 627032-Methylbuta-1,3-diene--2-methylprop-1-ene (1/1)

시약·촉매·용매 1

HCID 5943Carbon Tetrachloride용매

반응 조건

온도
75 °C

실험 절차

A 3.5% solution of 10 g of poly(isobutylene-co-isoprene) was prepared in 96.5% of a 1:1 mixture of trimethylpentane and CCl4. The solution was purged with N2, heated to 75° C., 0.3 g of benzoyl peroxide was added, followed by 40 g of methylmethacrylate, added over a period of 1 hour. The polymerization was carried out for 16 hours with constant mechanical stirring. After cooling to room temperature, the cleaning procedure used was identical to that of Example 1.

후처리

  1. customThe solution was purged with N2
  2. addition0.3 g of benzoyl peroxide was added
  3. additionadded over a period of 1 hour
  4. temperatureAfter cooling to room temperature

출처 및 근거

ORD 기록
ord-d951b2b78e8b4edf9165641b535f0515
출처 데이터셋
uspto-grants-1987_02
특허 번호
US04644041

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