Trimethylsilanol → Hexamethyldisiloxane
반응식
[CH3:1][Si:2]([CH3:5])([CH3:4])[OH:3]>C(OCC)C>[CH3:1][Si:2]([O:3][Si:2]([CH3:5])([CH3:4])[CH3:1])([CH3:5])[CH3:4]참가 물질
3
시약·촉매·용매 1
실험 절차
This reaction proceeds slowly without diethylether but reacts faster at reflux temperatures. Trimethylsilanol is condensed during the HMDS distillation step to give HMDSO, which reacts as shown above.
후처리
- customreacts faster
- temperatureat reflux temperatures
- customcondensed
- distillationduring the HMDS distillation step
출처 및 근거
- ORD 기록
- ord-5481fd3911d649d58cd82ef099a34174
- 출처 데이터셋
- uspto-grants-1987_02
- 특허 번호
- US04644076
반응 노트
불러오는 중…