Trimethylsilanol → Hexamethyldisiloxane

HRID 236426

반응식

HRID 236426 반응식
[CH3:1][Si:2]([CH3:5])([CH3:4])[OH:3]>C(OCC)C>[CH3:1][Si:2]([O:3][Si:2]([CH3:5])([CH3:4])[CH3:1])([CH3:5])[CH3:4]

참가 물질

3

반응물 1

HCID 66110Trimethylsilanol

생성물 1

HCID 24764Hexamethyldisiloxane

시약·촉매·용매 1

HCID 3283Diethyl Ether용매

실험 절차

This reaction proceeds slowly without diethylether but reacts faster at reflux temperatures. Trimethylsilanol is condensed during the HMDS distillation step to give HMDSO, which reacts as shown above.

후처리

  1. customreacts faster
  2. temperatureat reflux temperatures
  3. customcondensed
  4. distillationduring the HMDS distillation step

출처 및 근거

ORD 기록
ord-5481fd3911d649d58cd82ef099a34174
출처 데이터셋
uspto-grants-1987_02
특허 번호
US04644076

연결된 노트

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