Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Amino-4,6-dimethoxy-1,3,5-triazine → N-[(4,6-Dimethoxy-1,3,5-triazin-2-yl)aminocarbonyl]-4-methyl-3-thiophenesulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Amino-4,6-dimethoxy-1,3,5-triazine | HCID 27840 | — |
| 반응물 | 4-Methyl-3-thiophenesulfonyl isocyanate | HCID 13203331 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | N-[(4,6-Dimethoxy-1,3,5-triazin-2-yl)aminocarbonyl]-4-methyl-3-thiophenesulfonamide | HCID 13203333 | 43.4% |
반응 단계
A solution of 2 g of 4-methyl-3-thiophenesulfonyl isocyanate was added to a suspension of 1.5 g of 2-amino-4,6-dimethoxy-1,3,5-triazine in 20 ml of tetrahydrofuran and the resulting mixture stirred for 16 hours at ambient temperature. The precipitate thus obtained was filtered off and recrystallized to yield 1.5 g of the desired product, m.p. 154°-156°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04645529 |
| 출처 데이터셋 | uspto-grants-1987_02 |
| ORD ID | ord-ea7f7df6ae594cd0a9c4241d69a009a9 |
| 출처 메모 | uspto-grants-1987_02 |