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llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
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Ammonia → ((S)-4-Amino-4-carbamoyl-butyl)-carbamic acid benzyl ester

HRID 2365541
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인쇄 미리보기

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HRID 2365541 반응식
CO[C:3](=[O:20])[C@@H:4]([NH2:19])[CH2:5][CH2:6][CH2:7][NH:8][C:9]([O:11][CH2:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)=[O:10].[NH3:21]>CO>[CH2:12]([O:11][C:9](=[O:10])[NH:8][CH2:7][CH2:6][CH2:5][C@H:4]([NH2:19])[C:3](=[O:20])[NH2:21])[C:13]1[CH:14]=[CH:15][CH:16]=[CH:17][CH:18]=1
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 2

HCID 222AmmoniaHCID 7018807Methyl (S)-2-amino-5-(((benzyloxy)carbonyl)amino)pentanoate

생성물 1

HCID 67086977((S)-4-Amino-4-carbamoyl-butyl)-carbamic acid benzyl ester

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

(S)-2-Amino-5-benzyloxycarbonylamino-pentanoic acid methyl ester (2.80 g, 9.99 mmol) and 7M NH3 in MeOH (20 ml) is stirred at room temperature for 72 hours. The reaction mixture is evaporated to dryness in vacuo to yield a white solid. The white solid is suspended in diethyl ether before filtration and drying to yield ((S)-4-Amino-4-carbamoyl-butyl)-carbamic acid benzyl ester.

후처리

  1. customThe reaction mixture is evaporated to dryness in vacuo
  2. customto yield a white solid
  3. filtrationThe white solid is suspended in diethyl ether before filtration
  4. customdrying

출처 및 근거

ORD 기록
ord-62f252bf90224dc9bf3d9e813a45c42a
출처 데이터셋
uspto-grants-2014_04
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US08697687B2

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