Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Carbamic acid, [3-(bromoacetyl)phenyl]-, ethyl ester → HCID 178419570, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Carbamic acid, [3-(bromoacetyl)phenyl]-, ethyl ester | HCID 20216369 | — |
| 반응물 | HCID 178513045 | HCID 178513045 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 178419570 | HCID 178419570 | 94.9% |
반응 단계
A mixture of 17.17 gm of ethyl N-[3-(2-bromoacetyl)-phenyl]-carbamate, 7.1 gm of amidinothiourea and 45 ml of ethanol was refluxed for 4 hours and then cooled to room temperature. The precipitate formed thereby was filtered off and washed with cold ethanol, yielding 22 gm of the title compound, m.p. 240°-2° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04645841 |
| 출처 데이터셋 | uspto-grants-1987_02 |
| ORD ID | ord-6d885af43e5a42df8c8026180f6c9d4f |
| 출처 메모 | uspto-grants-1987_02 |