3,4-Dimethoxybenzeneacetonitrile → HCID 11964784, 화합물

HRID 2366439

반응식

HRID 2366439 반응식
[CH:1]1[C:14]2[CH:13]=[C:12]([CH:15]=O)[C:11]3[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=3)[C:5]=2[CH:4]=[CH:3][CH:2]=1.[CH3:17][O:18][C:19]1[CH:20]=[C:21]([CH:25]=[CH:26][C:27]=1[O:28][CH3:29])[CH2:22][C:23]#[N:24]>>[CH3:17][O:18][C:19]1[CH:20]=[C:21](/[C:22](=[CH:15]/[C:12]2[C:11]3[C:6]([C:5]4[CH:4]=[CH:3][CH:2]=[CH:1][C:14]=4[CH:13]=2)=[CH:7][CH:8]=[CH:9][CH:10]=3)/[C:23]#[N:24])[CH:25]=[CH:26][C:27]=1[O:28][CH3:29]

참가 물질

3

반응물 2

HCID 667273,4-DimethoxybenzeneacetonitrileHCID 78437Phenanthrene-9-carbaldehyde

생성물 1

HCID 11964784HCID 11964784, 화합물수율 63%

실험 절차

Phenanthrene-9-aldehyde (250 mg) was condensed with 3,4-dimethoxybenzyl cyanide (214 mg) through Method A (production step 2), to thereby yield the target product (yield: 278 mg, 63%).

출처 및 근거

ORD 기록
ord-6fae2bfe641e4e7e920b97f5be6c9f0d
출처 데이터셋
uspto-grants-2014_04
특허 번호
US08697742B2

연결된 노트

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