Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → HCID 178512607, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | 2-Bromo-2'-nitroacetophenone | HCID 244025 | — |
| 반응물 | HCID 178513045 | HCID 178513045 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | HCID 178512607 | HCID 178512607 | 95% |
반응 단계
A solution of 16.5 gm of 2-nitro-phenacyl bromide and 7.98 gm of amidinothiourea in 70 ml of dimethylformamide was stirred at room temperature for 16 hours, and then poured into 350 ml of water. The solution was made alkaline with 10% sodium hydroxide, and the solid which separated out after cooling was filtered, washed with water and dried, yielding 16.9 gm of the title compound, m.p. 176°-178° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04645841 |
| 출처 데이터셋 | uspto-grants-1987_02 |
| ORD ID | ord-0999f81bbcdc4f8fac59951338ee04e7 |
| 출처 메모 | uspto-grants-1987_02 |