참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1,3-Butadiene | HCID 7845 | — |
| 반응물 | Sulfolane | HCID 31347 | — |
| 생성물 | 3-Buten-2-ol | HCID 11716 | 60% |
| 생성물 | 2-Buten-1-ol | HCID 20024 | 26% |
반응 단계
In accordance with Example 1, a homogeneous solution of 6.2 grams (0.11 moles) of butadiene and 100 milliliters of a 65 volume percent aqueous sulfolane solution were reacted in the presence of a cation exchanger sold under the trademark Lewatit SPC 118 at a temperature of 100° C. After agitating at 100° C. for 6 hours, 76 percent of the mixture had reacted. A yield of 60 percent 1-butene-3-ol and a yield of 26 percent 2-butene-1-ol (crotylalcohol) was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04645863 |
|---|
| 출처 데이터셋 | uspto-grants-1987_02 |
|---|
| ORD ID | ord-aa74cbbdce7045b8b53dc7029ba5d8d2 |
|---|
| 출처 메모 | uspto-grants-1987_02 |
|---|
