Acrolein → 3-Oxa-tricyclo[6.2.1.02,7]undec-4-ene

참여 물질

역할	이름	HCID	투입량
반응물	Acrolein	HCID 7847	—
반응물	2-Norbornene	HCID 10352	—
촉매	Hydroquinone	HCID 785	—
생성물	3-Oxa-tricyclo[6.2.1.02,7]undec-4-ene	HCID 13539909	50%

반응 단계

56.4 g of norbornene, 16.8 g of acrolein and 0.5 g of hydroquinone were heated 15 hours at 190° in a stainless steel autoclave (pressure about 15 atm.). After evaporation a fractional distillation of the residue gave 22.5 g (yield 49%) of 3-oxa-tricyclo[6.2.1.02,7 ]undec-4-ene; b.p. 35°-7°/0.5 Torr.

출처 및 근거

DOI	10.6084/m9.figshare.5104873.v1
특허 번호	US04159258
출처 데이터셋	uspto-grants-1979_06
ORD ID	ord-efa0042304f54649aed1f9382912908e
출처 메모	uspto-grants-1979_06