HCID 20304516, 화합물 → HCID 20304565, 화합물

HRID 236960노트

반응식

HRID 236960 반응식
[CH2:1]([C:4]1[C:13]2[O:14][C:15]([C:20]([O:22][CH2:23][CH3:24])=[O:21])=[C:16]([CH3:19])[C:17](=[O:18])[C:12]=2[CH:11]=[C:10]2[C:5]=1[CH2:6][CH2:7][CH2:8][CH2:9]2)[CH:2]=[CH2:3]>[Pd]>[CH3:19][C:16]1[C:17](=[O:18])[C:12]2[CH:11]=[C:10]3[C:5]([CH2:6][CH2:7][CH2:8][CH2:9]3)=[C:4]([CH2:1][CH2:2][CH3:3])[C:13]=2[O:14][C:15]=1[C:20]([O:22][CH2:23][CH3:24])=[O:21]

참가 물질

3

반응물 1

HCID 20304516HCID 20304516, 화합물

생성물 1

HCID 20304565HCID 20304565, 화합물수율 100.6%

시약·촉매·용매 1

HCID 23938Palladium촉매

실험 절차

The product of step (e) (16 g) was hydrogenated over palladium on charcoal catalyst, under the conditions of Example 3(b), to give the title ester (16.2 g), as a low melting brown solid.

출처 및 근거

ORD 기록
ord-c92129996c0c460eb81fe32b3fcb7823
출처 데이터셋
uspto-grants-1979_06
특허 번호
US04159273

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