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Sodium Bicarbonate → HCID 23716997, 화합물

HRID 236962
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HRID 236962 반응식
C(=O)(O)[O-].[Na+:5].[CH3:6][C:7]1[C:8](=[O:27])[C:9]2[CH:23]=[C:22]3[C:17]([CH2:18][CH2:19][CH2:20][CH2:21]3)=[C:16]([CH2:24][CH2:25][CH3:26])[C:10]=2[O:11][C:12]=1[C:13]([OH:15])=[O:14]>O>[CH3:6][C:7]1[C:8](=[O:27])[C:9]2[CH:23]=[C:22]3[C:17]([CH2:18][CH2:19][CH2:20][CH2:21]3)=[C:16]([CH2:24][CH2:25][CH3:26])[C:10]=2[O:11][C:12]=1[C:13]([O-:15])=[O:14].[Na+:5]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 2

HCID 516892Sodium BicarbonateHCID 20304505HCID 20304505, 화합물

생성물 1

HCID 23716997HCID 23716997, 화합물

시약·촉매·용매 1

HCID 962Water용매

실험 절차

A solution of sodium bicarbonate (0.78 g) in water (30 ml) was added to the product of step (g) (2.8 g). The resulting solution was filtered then evaporated to small volume and diluted with acetone. Crystallisation occurred and the resulting crystals were filtered off and recovered as an off-white solid, which was the desired sodium salt (2.65 g).

후처리

  1. filtrationThe resulting solution was filtered
custom
then evaporated to small volume
  • additiondiluted with acetone
  • customCrystallisation
  • filtrationthe resulting crystals were filtered off
  • customrecovered as an off-white solid, which
  • 출처 및 근거

    ORD 기록
    ord-105ae161a11e4b6f801ee3bdf9499cea
    출처 데이터셋
    uspto-grants-1979_06
    DOI
    10.6084/m9.figshare.5104873.v1
    특허 번호
    US04159273

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