Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → alpha-D-Mannopyranose
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | alpha-Mannose phenylaminocyclobutenedione | HCID 86678081 | — |
| 용매 | Ethanol | HCID 702 | — |
| 용매 | Water | HCID 962 | — |
| 용매 | Water ethanol | HCID 19096565 | — |
| 생성물 | alpha-D-Mannopyranose | HCID 185698 | — |
반응 단계
Nanoparticles DB052 (200 mg) were stirred up by ultrasounds for 30 minutes in ethanol (5 mL). α-mannose phenylaminocyclobutenedione derivatives (71 mg, 1.8 10−4 mol, structure here above) was dissolved in an ethanol/water mixture (10 ml, 3/2). The α-mannose phenylaminocyclobutenedione derivative solution was added dropwisely to the nanoparticle suspension. Triethylamine (500 μL) was added, and the suspension was stirred for 18 hours. After centrifugation, the nanoparticles were dispersed in water and centrifuged (3 cycles), then dispersed in ethanol and centrifugated (two cycles). Functionalized nanoparticles (DB069) were obtained (200 mg).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08709747B2 |
| 출처 데이터셋 | uspto-grants-2014_04 |
| ORD ID | ord-d956c0b2d6f44e7aad3939dd97a400b7 |
| 출처 메모 | uspto-grants-2014_04 |