Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Furoin → HCID 178527844, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Furoin | HCID 11100 | — |
| 반응물 | Ammonium thiocyanate | HCID 15666 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 178527844 | HCID 178527844 | 49.1% |
반응 단계
α-Furoin (19.2 g; 0.1 mole) was reacted with 11.5 g (0.15 mole) ammonium thiocyanate in ethanol heated at reflux to afford 11.4 g of 4,5-bis-(2-furyl)-1H-2-imidazolethiol. An analytical sample was prepared by chromatography on alumina with ethanol and recrystallization from nitromethane, m.p. 279°-380° (dec.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04159338 |
| 출처 데이터셋 | uspto-grants-1979_06 |
| ORD ID | ord-65eab635b120478aa7c2e0cef350716f |
| 출처 메모 | uspto-grants-1979_06 |