HCID 46944971, 화합물 → HCID 46944972, 화합물

HRID 2370590노트

반응식

HRID 2370590 반응식
[CH3:1][C:2]1([CH3:43])[N:6]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][S:16]([CH2:18][CH2:19]CC(F)(F)C(F)(F)F)=[O:17])[C:5](=[O:28])[N:4]([C:29]2[CH:34]=[CH:33][C:32]([N+:35]([O-:37])=[O:36])=[C:31]([C:38]([F:41])([F:40])[F:39])[CH:30]=2)[C:3]1=[O:42].CC1(C)N(CCCCCCCCCSCC[C:62]([F:74])([F:73])[C:63]([F:72])([F:71])[C:64]([F:70])([F:69])[C:65]([F:68])([F:67])[F:66])C(=O)N(C2C=CC([N+]([O-])=O)=C(C(F)(F)F)C=2)C1=O>>[CH3:1][C:2]1([CH3:43])[N:6]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][S:16]([CH2:18][CH2:19][C:62]([F:74])([F:73])[C:63]([F:71])([F:72])[C:64]([F:69])([F:70])[C:65]([F:68])([F:67])[F:66])=[O:17])[C:5](=[O:28])[N:4]([C:29]2[CH:34]=[CH:33][C:32]([N+:35]([O-:37])=[O:36])=[C:31]([C:38]([F:39])([F:41])[F:40])[CH:30]=2)[C:3]1=[O:42]

참가 물질

3

반응물 2

HCID 46944971HCID 46944971, 화합물HCID 46947540HCID 46947540, 화합물

생성물 1

HCID 46944972HCID 46944972, 화합물수율 85%

실험 절차

The experimental protocol used is the same as that described for the synthesis of the compound of Example 2, the compound of Example 14 replacing the compound of Example 1. A pale yellow oil is obtained with a yield of 85% (145 mg).

후처리

  1. customA pale yellow oil is obtained with a yield of 85% (145 mg)

출처 및 근거

ORD 기록
ord-91463e120e5b486687652ee19ef089a5
출처 데이터셋
uspto-grants-2014_04
특허 번호
US08710091B2

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