Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Acetate → 7-(alpha,alpha,alpha-Trifluoro-m-tolyl)-1,2,4-triazolo[4,3-b]-1,2,4-triazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Acetate | HCID 517045 | — |
| 반응물 | 3,4-Diamino-1,2,4-triazole | HCID 567144 | — |
| 반응물 | 3-(Trifluoromethyl)phenylglyoxal | HCID 2783284 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | 7-(alpha,alpha,alpha-Trifluoro-m-tolyl)-1,2,4-triazolo[4,3-b]-1,2,4-triazine | HCID 12581259 | — |
반응 단계
A solution of 12.5 g. of m-trifluoromethylphenylglyoxal, 7.69 g. of 3,4-diamino-4H-1,2,4-triazole and 4.67 g. of sodium acetate in 120 ml. of 67% acetic acid is reacted as described in Example 4, giving the desired product as a yellow solid, m.p. 288°-290° C. (dec.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04159375 |
| 출처 데이터셋 | uspto-grants-1979_06 |
| ORD ID | ord-f4851c6324344971a5eec2736d4ea614 |
| 출처 메모 | uspto-grants-1979_06 |