Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl (R)-(1-hydroxy-3-methylbutan-2-YL)carbamate → (4R)-4-(Propan-2-yl)-1,3-oxazolidin-2-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl (R)-(1-hydroxy-3-methylbutan-2-YL)carbamate | HCID 15714133 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | (4R)-4-(Propan-2-yl)-1,3-oxazolidin-2-one | HCID 641505 | — |
반응 조건
| 온도 | 150 °C |
|---|
반응 단계
27.2 g (168.7 mmol) of the compound from Example V are dissolved in 400 ml of toluene and stirred under reflux in an oil bath at 150° C. while passing in nitrogen.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05095006 |
| 출처 데이터셋 | uspto-grants-1992_03 |
| ORD ID | ord-7518c1e32d2b4d4fadb76a3e57559c1e |
| 출처 메모 | uspto-grants-1992_03 |