Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 3-benzyl-2-[(N-cyclohexylcarbamoyl)-imino]benzothiazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Cyclohexyl isocyanate | HCID 18502 | — |
| 반응물 | 3-Benzyl-2-iminobenzothiazole | HCID 677566 | — |
| 반응물 | Di-n-butyldilauryltin | HCID 9809426 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | 3-benzyl-2-[(N-cyclohexylcarbamoyl)-imino]benzothiazole | HCID 54467310 | 73.1% |
반응 단계
To a solution of 1.8 g of 3-benzyl-2-iminobenzothiazole and a catalytic amount of dibutyltin dilaurate in 30 ml of acetone was added 0.95 g of cyclohexyl isocyanate dropwise. After seven hours, the reaction mixture was poured into approximately 100 ml of water. The crystals precipitated were collected by filtering to thereby obtain 2.0 g of the objective compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05095025 |
| 출처 데이터셋 | uspto-grants-1992_03 |
| ORD ID | ord-0e6b3d4aa3dc4c98960b65ff1deb1b73 |
| 출처 메모 | uspto-grants-1992_03 |