Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Aniline → 3-Phenylammonio-1-propanesulfonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Aniline | HCID 6115 | — |
| 반응물 | Propane sultone | HCID 14264 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | 3-Phenylammonio-1-propanesulfonate | HCID 12546060 | 95% |
반응 단계
A mixture of aniline (7 mmol) and propane sultone (10 mmol) was heated in 10 mL of acetonitrile at 12.0-130° C. for 9 h in a pressure tube under argon atmosphere. The product was allowed to cool to room temperature and the solid of 3-phenylammonio-1-propanesulfonate was filtered and air-dried. Yield: 95%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08642014B2 |
| 출처 데이터셋 | uspto-grants-2014_02 |
| ORD ID | ord-f03ab8001ee74a3fa69d20bb82c32bc4 |
| 출처 메모 | uspto-grants-2014_02 |