Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 2-((Benzyloxy)methyl)-2-ethylpropane-1,3-diol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | 5-Benzyloxymethyl-2,2-dimethyl-5-ethyl-1,3-dioxane | HCID 19904400 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 2-((Benzyloxy)methyl)-2-ethylpropane-1,3-diol | HCID 53806630 | — |
반응 단계
5-Benzyloxymethyl-2,2-dimethyl-5-ethyl-1,3-dioxane (15.0 g.) and Dowex 50×8-200 ion exchange resin (H+ form) (2.0 g.) in methanol (250ml.) containing water (50 ml.) was refluxed, with stirring, for three hours. The mixture was filtered and the filtrate was evaporated in vacuo. 2-Benzyloxymethyl-2-hydroxymethyl-butan-1-ol was obtained as a yellow oil (9.7 g.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05098929 |
| 출처 데이터셋 | uspto-grants-1992_03 |
| ORD ID | ord-71d753a6e4514cb2b1b5cad200a2bf4d |
| 출처 메모 | uspto-grants-1992_03 |