Thionyl Chloride → 4-(Chlorocarbonyl)phenyl nonanoate
반응식
[CH2:1]([C:9]([O:11][C:12]1[CH:20]=[CH:19][C:15]([C:16](O)=[O:17])=[CH:14][CH:13]=1)=[O:10])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].S(Cl)([Cl:23])=O>C(Cl)(Cl)(Cl)Cl>[CH2:1]([C:9]([O:11][C:12]1[CH:20]=[CH:19][C:15]([C:16]([Cl:23])=[O:17])=[CH:14][CH:13]=1)=[O:10])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]참가 물질
4
실험 절차
2.5 g of 4-octylcarbonyloxybenzoic acid was dispersed in 50 ml carbon tetrachloride, after dropping 10 ml of thionyl chloride to this solution, refluxed for three hours. After reducing the solvent, 4-octylcarbonyloxybenzoic chloride (CK) was obtained.
후처리
- temperaturerefluxed for three hours
출처 및 근거
- ORD 기록
- ord-9798d60ffc9a4a22a11c8ca7d6213637
- 출처 데이터셋
- uspto-grants-1992_03
- 특허 번호
- US05100579
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