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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 2373443생성일: 2026년 10월 26일

1-(4-Iodophenyl)ethan-1-one → 1-[4-(3,3-Dimethyl-3,4-dihydro-2H-benzo[b][1,4]dioxepin-7-ylethynyl)-phenyl]-ethanone

https://huagongshe.com/reaction/2373443

반응식

참여 물질

역할이름HCID투입량
반응물1-(4-Iodophenyl)ethan-1-oneHCID 72869—
반응물7-Ethynyl-3,3-dimethyl-3,4-dihydro-2H-benzo[b][1,4]dioxepineHCID 59852695—
생성물1-[4-(3,3-Dimethyl-3,4-dihydro-2H-benzo[b][1,4]dioxepin-7-ylethynyl)-phenyl]-ethanoneHCID 59852693—

반응 단계

The title compound is prepared in analogy to example 1 from 7-ethynyl-3,3-dimethyl-3,4-dihydro-2H-benzo[b][1,4]dioxepine (6) (example 1d) and 1-(4-iodo-phenyl)-ethanone. MS (ESI) 320.2 (M•)+.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07459480B2
출처 데이터셋uspto-grants-2008_12
ORD IDord-fbe8ec5045bd41b1b9a90e85259d1044
출처 메모uspto-grants-2008_12