Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-Iodo-2,3-dihydro-1-benzofuran → 7-(2,3-Dihydro-benzofuran-5-ylethynyl)-3,3-dimethyl-3,4-dihydro-2H-benzo[b][1,4]dioxepine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-Iodo-2,3-dihydro-1-benzofuran | HCID 2736133 | — |
| 반응물 | 7-Ethynyl-3,3-dimethyl-3,4-dihydro-2H-benzo[b][1,4]dioxepine | HCID 59852695 | — |
| 생성물 | 7-(2,3-Dihydro-benzofuran-5-ylethynyl)-3,3-dimethyl-3,4-dihydro-2H-benzo[b][1,4]dioxepine | HCID 69291311 | — |
반응 단계
The title compound is prepared in analogy to example 1 from 7-ethynyl-3,3-dimethyl-3,4-dihydro-2H-benzo[b][1,4]dioxepine (6) (example 1d) and 5-iodo-2,3-dihydro-benzofuran. MS (ESI) 320.1 (M•)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07459480B2 |
| 출처 데이터셋 | uspto-grants-2008_12 |
| ORD ID | ord-e95819f62fb64fe58f613dcd60496791 |
| 출처 메모 | uspto-grants-2008_12 |