Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-(1-Acetylpiperidin-4-yl)propanoic acid → 9-[3-(1-Acetyl-4-piperidinyl)propanoyl]-2,3,6,7-tetrahydro-1H,5H-pyrido[3,2,1-ij]quinolin-5-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-(1-Acetylpiperidin-4-yl)propanoic acid | HCID 9855751 | — |
| 반응물 | 1,2,6,7-tetrahydro-5H-pyrido[3,2,1-ij]quinolin-3-one | HCID 13694564 | — |
| 생성물 | 9-[3-(1-Acetyl-4-piperidinyl)propanoyl]-2,3,6,7-tetrahydro-1H,5H-pyrido[3,2,1-ij]quinolin-5-one | HCID 21887765 | — |
반응 단계
Using 3-(1-acetyl-4-piperidinyl)propanoic acid (13.8 g) and 2,3,6,7-tetrahydro-1H,5H-pyrido[3,2,1-ij]quinolin-5-one (10.8 g) according to the same method as that of Reference Example 172, the title compound was obtained as colorless crystals (15.5 g) having a melting point of 130 to 131° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07462628B2 |
| 출처 데이터셋 | uspto-grants-2008_12 |
| ORD ID | ord-e08fc3af4ab449f2a6798eb5b3edee5d |
| 출처 메모 | uspto-grants-2008_12 |