Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 237613생성일: 2026년 10월 25일
6-Chloro-2-methyl-2,3-dihydropyridazin-3-one → 6-(4-Amino-3,5-dimethylphenyl)-2-methylpyridazin-3(2H)-one
https://huagongshe.com/reaction/237613
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 6-Chloro-2-methyl-2,3-dihydropyridazin-3-one | HCID 2783607 | — |
| 반응물 | 2,6-Dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline | HCID 56737724 | — |
| 생성물 | 6-(4-Amino-3,5-dimethylphenyl)-2-methylpyridazin-3(2H)-one | HCID 86697284 | — |
반응 단계
The title compound is prepared from 6-chloro-2-methylpyridazin-3(2H)-one and 2,6-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline following a procedure analogous to that described in Step 2 of Intermediate 62. The mixture is stirred for 12 hours at 60° C. LC (method 9): tR=0.78 min; Mass spectrum (ESI+): m/z=230 [M+H]+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US08642585B2 |
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| 출처 데이터셋 | uspto-grants-2014_02 |
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| ORD ID | ord-83d92abcc37f4bf3b06641409de7fa4a |
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| 출처 메모 | uspto-grants-2014_02 |
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