2-Iodobenzaldehyde → HCID 21099432, 화합물

반응식

I[C:2]1[CH:9]=[CH:8][CH:7]=[CH:6][C:3]=1[CH:4]=[O:5].[F:10][C:11]1[CH:16]=[C:15]([F:17])[CH:14]=[CH:13][C:12]=1[CH2:18][CH2:19][C:20]1[CH:25]=[CH:24][C:23]([S:26](C2C=CC=CC=2)(=[O:28])=[O:27])=[CH:22][CH:21]=1>>[F:10][C:11]1[CH:16]=[C:15]([F:17])[CH:14]=[CH:13][C:12]=1/[CH:18]=[CH:19]/[C:20]1[CH:25]=[CH:24][C:23]([S:26]([C:2]2[CH:9]=[CH:8][CH:7]=[CH:6][C:3]=2[CH:4]=[O:5])(=[O:28])=[O:27])=[CH:22][CH:21]=1

참가 물질

반응물 2

HCID 6434392-Iodobenzaldehyde

HCID 21099424HCID 21099424, 화합물

생성물 1

HCID 21099432HCID 21099432, 화합물

실험 절차

2-({4-[(E)-2-(2,4-difluorophenyl)vinyl]phenyl}sulfonyl)benzaldehyde was prepared according to the method of Example 135, Step 2 using 2-iodobenzaldehyde in place of (S)-1-(2-iodophenyl)ethanol and Intermediate 2 in place of Intermediate 1.

출처 및 근거

ORD 기록: ord-0d687b06d30c4131818f45abc296fb4b
출처 데이터셋: uspto-grants-2008_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07468393B2

반응 노트

불러오는 중…