Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Methyl-2-cyclohexen-1-one → 3-Methyl-2-cyclohexen-1-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Methyl-2-cyclohexen-1-one | HCID 14511 | — |
| 반응물 | HCID 178418373 | HCID 178418373 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | 3-Methyl-2-cyclohexen-1-one | HCID 14511 | — |
| 생성물 | Cyclohexanone, 3,3-dimethyl- | HCID 76322 | — |
반응 단계
First, 3-methyl-cyclohexenone was prepared in accordance with the procedures of Jirgensons et. al., Euro. J. Med. Chem. 35 (2000) 555-565. Then, 3-methyl-cyclohexenone was reacted with methyl magnesium iodide in the presence of cuprous chloride in diethyl ether to obtain the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08642603B2 |
| 출처 데이터셋 | uspto-grants-2014_02 |
| ORD ID | ord-f2ed5d56b2764e25bcbeb6e69c3a3e53 |
| 출처 메모 | uspto-grants-2014_02 |