1-Naphthalenemethanamine → HCID 62368325, 화합물

HRID 2378084노트

반응식

HRID 2378084 반응식
[NH2:1][CH2:2][C:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[CH:6]=[CH:5][CH:4]=1.[NH:13]([C:15](=[O:20])[C:16](OC)=[O:17])[NH2:14]>CO>[NH:13]([C:15](=[O:20])[C:16]([NH:1][CH2:2][C:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[CH:6]=[CH:5][CH:4]=1)=[O:17])[NH2:14]

참가 물질

4

반응물 2

HCID 83551-NaphthalenemethanamineHCID 11355473Methyl hydrazino(oxo)acetate

생성물 1

HCID 62368325HCID 62368325, 화합물

시약·촉매·용매 1

HCID 887Methanol용매2회

실험 절차

1.25 ml 1-aminomethylnaphthalene are added to a solution of 1.0 g methyl hydrazino-oxo-acetate in 10 ml of methanol. The solution is stirred for 16 h at ambient temperature and then some of the methanol is eliminated. The precipitate is separated off, washed with diethyl ether, and dried.

후처리

  1. customThe precipitate is separated off
  2. washwashed with diethyl ether
  3. customdried

출처 및 근거

ORD 기록
ord-2ed23cf9f90c44a0b2d2e202c25b93bd
출처 데이터셋
uspto-grants-2008_12
특허 번호
US07470716B2

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