(4-Methoxyphenyl)boronic acid → 4-(3,3,5,5-Tetramethyl-cyclohexyl)-phenol

HRID 237851노트

반응식

HRID 237851 반응식
C[O:2][C:3]1[CH:8]=[CH:7][C:6](B(O)O)=[CH:5][CH:4]=1.[CH3:12][C:13]1([CH3:29])[CH2:18][C:17]([CH3:20])([CH3:19])[CH2:16][C:15](OS(C(F)(F)F)(=O)=O)=[CH:14]1>>[CH3:12][C:13]1([CH3:29])[CH2:18][C:17]([CH3:20])([CH3:19])[CH2:16][CH:15]([C:6]2[CH:7]=[CH:8][C:3]([OH:2])=[CH:4][CH:5]=2)[CH2:14]1

참가 물질

3

반응물 2

HCID 201262(4-Methoxyphenyl)boronic acidHCID 110873803,3,5,5-Tetramethylcyclohex-1-en-1-yl triflate

생성물 1

HCID 685258634-(3,3,5,5-Tetramethyl-cyclohexyl)-phenol

실험 절차

The title compound was prepared from 4-methoxy-benzeneboronic acid and trifluoro-methanesulfonic acid 3,3,5,5-tetramethyl-cyclohex-1-enyl ester in accordance with the procedure described in Step 1, Example 86.

출처 및 근거

ORD 기록
ord-6977e0eeff3649f4a53ceae7dd33409a
출처 데이터셋
uspto-grants-2014_02
특허 번호
US08642603B2

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