Ethyl chloroformate → 4-Ethylsulfanyl-but-2-ynoic acid ethyl ester

HRID 237872노트

반응식

[CH2:1]([S:3][CH2:4][C:5]#[CH:6])[CH3:2].Cl[C:8]([O:10][CH2:11][CH3:12])=[O:9]>>[CH2:11]([O:10][C:8](=[O:9])[C:6]#[C:5][CH2:4][S:3][CH2:1][CH3:2])[CH3:12]

참가 물질

반응물 2

HCID 10928Ethyl chloroformate

HCID 5224803-(Ethylsulfanyl)prop-1-yne

생성물 1

HCID 866402404-Ethylsulfanyl-but-2-ynoic acid ethyl ester

실험 절차

The title compound was prepared from 3-ethylsulfanyl-propyne and ethyl chloroformate in accordance with the procedures of G. Cai et al., Tetrahedron, 2006, (5697-5708).

출처 및 근거

ORD 기록: ord-9dd0bf252f9a4139ab826dc7e0ebc9dd
출처 데이터셋: uspto-grants-2014_02
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08642603B2

반응 노트

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