Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 4'-n-Decylbiphenyl-4-carboxylic acid chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 4'-n-Decyl-4-carboxybiphenyl | HCID 11405011 | — |
| 생성물 | 4'-n-Decylbiphenyl-4-carboxylic acid chloride | HCID 54012389 | — |
반응 단계
After 4'-n-decyl-4-carboxybiphenyl (3.10 g) was heated under reflux for 6 hours together with an excessive amount of thionyl chloride, unaltered thionyl chloride was removed by distillation to give about 3 g of 4'-n-decylbiphenyl-4-carboxylic acid chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05364561 |
| 출처 데이터셋 | uspto-grants-1994_11 |
| ORD ID | ord-268bbd2b02cb424aa986af4ecfbef9e9 |
| 출처 메모 | uspto-grants-1994_11 |