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Water → HCID 67790522, 화합물

HRID 2380562
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인쇄 미리보기

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HRID 2380562 반응식
[CH:1]([C:4]1[C:5]([O:16][CH3:17])=[C:6]([CH:10]=[C:11]([CH:13]([CH3:15])[CH3:14])[CH:12]=1)[C:7]([OH:9])=[O:8])([CH3:3])[CH3:2].[OH-].[K+].O.O.O.O.O.O.O.O.S([O-])([O-])(=O)=O.[Zn+2:33]>CO>[CH:1]([C:4]1[C:5]([O:16][CH3:17])=[C:6]([CH:10]=[C:11]([CH:13]([CH3:15])[CH3:14])[CH:12]=1)[C:7]([O-:9])=[O:8])([CH3:3])[CH3:2].[Zn+2:33].[CH:1]([C:4]1[C:5]([O:16][CH3:17])=[C:6]([CH:10]=[C:11]([CH:13]([CH3:15])[CH3:14])[CH:12]=1)[C:7]([O-:9])=[O:8])([CH3:3])[CH3:2]
참가 물질반응 조건실험 절차후처리출처 및 근거반응 노트

참가 물질

6

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HCID 962Water2회HCID 14797Potassium HydroxideHCID 62640Zinc Sulfate HeptahydrateHCID 189545872-Methoxy-3,5-di(propan-2-yl)benzoic acid

생성물 1

HCID 67790522HCID 67790522, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

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온도
60 °C

실험 절차

Five parts of 3,5-diisopropyl-2-methoxybenzoic acid was dissolved in 80 parts of methyl alcohol, followed by the addition of an aqueous solution of 1.3 parts of 96% potassium hydroxide in 10 parts of water. The resulting mixture was heated to 60° C. An aqueous solution of 3.2 parts of zinc sulfate heptahydrate in 10 parts of water was dropped into the resulting mixture over a period of 15 minutes. After the completion of the dropping, the obtained mixture was stirred at that temperature for 2 hours, cooled to a room temperature and filtered to recover a white crystalline precipitate. This precipitate was dispersed in 60 parts of water, washed therewith and filtered. The obtained filter cake was dried to give 4.8 parts of a white crystal. The melting point thereof was 104 to 107° C.

후처리

  1. temperaturecooled to a room temperature
  2. filtrationfiltered
  3. customto recover a white crystalline precipitate
  4. additionThis precipitate was dispersed in 60 parts of water
  5. washwashed
  6. filtrationfiltered
  7. filtrationThe obtained filter cake
  8. customwas dried
  9. customto give 4.8 parts of a white crystal
  10. customthereof was 104 to 107° C.

출처 및 근거

ORD 기록
ord-be9b6bc0429c4fb4a61a7f4d75c9dabe
출처 데이터셋
uspto-grants-1994_11
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US05368971

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