HCID 59443055, 화합물 → HCID 59443022, 화합물

HRID 2380900노트

반응식

HRID 2380900 반응식
Br[C:2]1[C:3]([CH3:21])([CH3:20])[O:4][C:5]2[C:10]([C:11]=1[C:12]1[CH:17]=[CH:16][C:15]([F:18])=[CH:14][CH:13]=1)=[CH:9][CH:8]=[C:7]([Cl:19])[CH:6]=2>C([Sn](CCCC)(CCCC)C=C)CCC>[Cl:19][C:7]1[CH:6]=[C:5]2[C:10]([C:11]([C:12]3[CH:17]=[CH:16][C:15]([F:18])=[CH:14][CH:13]=3)=[C:2]([C:3]([O:4][CH2:5][CH3:6])=[CH2:2])[C:3]([CH3:21])([CH3:20])[O:4]2)=[CH:9][CH:8]=1

참가 물질

3

반응물 1

HCID 59443055HCID 59443055, 화합물

생성물 1

HCID 59443022HCID 59443022, 화합물

시약·촉매·용매 1

HCID 81998Tributylvinyltin용매

실험 절차

A mixture of 3-bromo-7-chloro-4-(4-fluorophenyl)-2,2-dimethyl-2H-chromen (a compound obtained in Reference Example 8(1); 220 mg) and tributyl(vinyl)tin (405 μL) were treated in the same manner as Reference Example 11(1) to give the titled compound (144 mg) as a pale yellow powder.

후처리

  1. customobtained in Reference Example 8(1)

출처 및 근거

ORD 기록
ord-9f465389bac74900ac6127e2e70ef081
출처 데이터셋
uspto-grants-2012_09
특허 번호
US08258131B2

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