Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,6-Dimethylaniline → N-(2,6-Dimethylphenyl)formamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,6-Dimethylaniline | HCID 6896 | — |
| 반응물 | Sodium Acetate | HCID 517045 | — |
| 용매 | Formic Acid | HCID 284 | — |
| 생성물 | N-(2,6-Dimethylphenyl)formamide | HCID 345859 | 79% |
반응 단계
4.1 10.0 g of sodium acetate are dissolved in 120 ml of formic acid. 50.0 g of 2,6-dimethylaniline 11 are then introduced, and the mixture is stirred under reflux for 24 h. The mixture is subsequently subjected to conventional work-up, giving 48.9 g (79%) of N-(2,6-dimethylphenyl)formamide 12; MS-EI (M+)=149.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08258151B2 |
| 출처 데이터셋 | uspto-grants-2012_09 |
| ORD ID | ord-ecafce52565e444bbd417d8c3ac09ba6 |
| 출처 메모 | uspto-grants-2012_09 |