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llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
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(RS)-S-(4-nitrophenyl)-N-(methylcarbamoyl)-S-methylsulfoximide → (RS)-S-(4-aminophenyl)-N-(methylcarbamoyl)-S-methylsulfoximide

HRID 238138
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인쇄 미리보기

반응식

HRID 238138 반응식
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([S:10]([CH3:17])(=[N:12][C:13](=[O:16])[NH:14][CH3:15])=[O:11])=[CH:6][CH:5]=1)([O-])=O>CO.[Pd]>[NH2:1][C:4]1[CH:9]=[CH:8][C:7]([S:10]([CH3:17])(=[N:12][C:13](=[O:16])[NH:14][CH3:15])=[O:11])=[CH:6][CH:5]=1
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 1

HCID 59550870(RS)-S-(4-nitrophenyl)-N-(methylcarbamoyl)-S-methylsulfoximide

생성물 1

HCID 59550841(RS)-S-(4-aminophenyl)-N-(methylcarbamoyl)-S-methylsulfoximide

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 887Methanol용매

실험 절차

302 mg (1.17 mmol) (RS)—S-(4-nitrophenyl)-N-(methylcarbamoyl)-S-methylsulfoximide in 20 ml methanol is hydrogenated over 60 mg palladium (10% on carbon, 50% water wet) for 4 hours at 26° C. and 30 bar. The catalyst is filtered and the solvent evaporated to give 271 mg (corresponding to 100% of theor.) of the product.

후처리

  1. filtrationThe catalyst is filtered
  2. customthe solvent evaporated
  3. customto give 271 mg (corresponding to 100% of theor.) of the product

출처 및 근거

ORD 기록
ord-960c30a9466b4919ad90f83963fd98bf
출처 데이터셋
uspto-grants-2014_02
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US08642611B2

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