1-methyl-5-(2-phenylethenyl)-1H-pyrazole → 1-Methyl-5-(2-phenylethyl)-1H-pyrazole

HRID 238359

반응식

HRID 238359 반응식
[CH3:1][N:2]1[C:6]([CH:7]=[CH:8][C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)=[CH:5][CH:4]=[N:3]1>[C].[Pd].C(O)C>[CH3:1][N:2]1[C:6]([CH2:7][CH2:8][C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)=[CH:5][CH:4]=[N:3]1

참가 물질

4

반응물 1

HCID 714019871-methyl-5-(2-phenylethenyl)-1H-pyrazole

생성물 1

HCID 866848621-Methyl-5-(2-phenylethyl)-1H-pyrazole수율 102.2%

시약·촉매·용매 2

HCID 178418390HCID 178418390, 화합물촉매HCID 702Ethanol용매

실험 절차

10% Palladium carbon (30 mg) was added to an ethanol (3.0 mL) solution of 1-methyl-5-(2-phenylethenyl)-1H-pyrazole (300 mg), and the obtained solution was then stirred under a hydrogen atmosphere at a room temperature for 14 hours. Thereafter, the reaction solution was filtrated with Celite, and the filtrate was then concentrated under a reduced pressure, so as to obtain the title compound (310 mg) in the form of a colorless oily substance.

후처리

  1. filtrationThereafter, the reaction solution was filtrated with Celite
  2. concentrationthe filtrate was then concentrated under a reduced pressure

출처 및 근거

ORD 기록
ord-50ee3e6cf35c4f86b305a317eca7ecc6
출처 데이터셋
uspto-grants-2014_02
특허 번호
US08642626B2

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