5-Bromosalicylic acid → 5-Bromo-N [3-bromo-5-(trifluoromethyl)phenyl]-2-hydroxybenzamide

HRID 2384404

반응식

HRID 2384404 반응식
[Br:1][C:2]1[CH:10]=[C:6]([C:7]([OH:9])=O)[C:5]([OH:11])=[CH:4][CH:3]=1.[Br:12][C:13]1[CH:14]=[C:15]([CH:17]=[C:18]([C:20]([F:23])([F:22])[F:21])[CH:19]=1)[NH2:16]>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]([OH:11])=[C:6]([CH:10]=1)[C:7]([NH:16][C:15]1[CH:17]=[C:18]([C:20]([F:21])([F:22])[F:23])[CH:19]=[C:13]([Br:12])[CH:14]=1)=[O:9]

참가 물질

3

반응물 2

HCID 69725-Bromosalicylic acidHCID 27358803-Bromo-5-(trifluoromethyl)aniline

생성물 1

HCID 178602635-Bromo-N [3-bromo-5-(trifluoromethyl)phenyl]-2-hydroxybenzamide수율 73.3%

실험 절차

Using 5-bromosalicylic acid and 3-bromo-5-(trifluoromethyl)aniline as the raw materials, the same operation as the example 16 gave the title compound.

출처 및 근거

ORD 기록
ord-09da93bd55dd4e09b2f0071d3bb6340f
출처 데이터셋
uspto-grants-2012_09
특허 번호
US08263657B2

연결된 노트

불러오는 중…