참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Ethylene Glycol | HCID 174 | — |
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Sodium Methoxide | HCID 10942334 | — |
| 반응물 | ethyl 3-(N-vinylformamido)propionate | HCID 19690337 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 2-hydroxyethyl 3-(N-vinylformamido)propionate | HCID 19690342 | — |
반응 단계
The apparatus of Example 2 was charged with 17.1 grams (0.1 mol) of ethyl 3-(N-vinylformamido)propionate, 6.2 grams (0.1 mol) of ethylene glycol, and 0.15 gram of 25% sodium methoxide in methanol solution. The mixture was stirred at 90° C. for 2 hours. No evolution of ethanol was observed during the reaction period. Heating for an additional hour at 135° C. also failed to generate a volatile coproduct which indicated no conversion to the desired product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05728878 |
|---|
| 출처 데이터셋 | uspto-grants-1998_03 |
|---|
| ORD ID | ord-9263fd3c38db4e7d8af1acf74087dcb3 |
|---|
| 출처 메모 | uspto-grants-1998_03 |
|---|
