참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Allylamine | HCID 7853 | — |
| 반응물 | Sodium Methoxide | HCID 10942334 | — |
| 반응물 | ethyl 3-(N-vinylformamido)propionate | HCID 19690337 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | N-allyl-3-(N-vinylformamido)propionamide | HCID 19690345 | — |
반응 단계
A 100mL stainless steel high pressure reactor was charged with 17.1 grams (0.1 mol) of ethyl 3-(N-vinylformamido)propionate, 5.7 grams (0.1 mol) of allylamine and 0.15 gram of 25% sodium methoxide in methanol solution. The mixture was heated at 90° C. for 3 hours. Subsequent NMR analysis of the reaction mixture showed no conversion of the starting materials.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05728878 |
|---|
| 출처 데이터셋 | uspto-grants-1998_03 |
|---|
| ORD ID | ord-e627c68d0c1743fc987ec32e90fb2b64 |
|---|
| 출처 메모 | uspto-grants-1998_03 |
|---|
