Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Bromo-2-methylpyridine → Tert-butyl{4-chloro-2-[(2-methylpyridin-3-yl)ethynyl]phenoxy}acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Bromo-2-methylpyridine | HCID 1201003 | — |
| 반응물 | Tert-butyl(4-chloro-2-ethynylphenoxy)acetate | HCID 56594381 | — |
| 생성물 | Tert-butyl{4-chloro-2-[(2-methylpyridin-3-yl)ethynyl]phenoxy}acetate | HCID 58521928 | — |
반응 단계
Following the general method as outlined in Intermediate 19, starting from tert-butyl(4-chloro-2-ethynylphenoxy)acetate (Intermediate 3) and 3-bromo-2-methylpyridine (Synchem-OHG), the title compound was obtained as a yellow sticky solid after purification by preparative HPLC.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08273769B2 |
| 출처 데이터셋 | uspto-grants-2012_09 |
| ORD ID | ord-ccbd8eec367c44b3b021eaff2794922d |
| 출처 메모 | uspto-grants-2012_09 |