5-(methylsulfonyl)-2-[(1E)-prop-1-en-1-yl]aniline → 5-(Methylsulfonyl)-2-propylaniline

HRID 2390157노트

반응식

HRID 2390157 반응식
[CH3:1][S:2]([C:5]1[CH:6]=[CH:7][C:8](/[CH:12]=[CH:13]/[CH3:14])=[C:9]([CH:11]=1)[NH2:10])(=[O:4])=[O:3].[H][H]>CO.[Pd]>[CH3:1][S:2]([C:5]1[CH:6]=[CH:7][C:8]([CH2:12][CH2:13][CH3:14])=[C:9]([CH:11]=1)[NH2:10])(=[O:3])=[O:4]

참가 물질

5

반응물 2

HCID 585220135-(methylsulfonyl)-2-[(1E)-prop-1-en-1-yl]aniline2회HCID 178418361HCID 178418361, 화합물

생성물 1

HCID 585220065-(Methylsulfonyl)-2-propylaniline

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 887Methanol용매

실험 절차

A mixture of 5-(methylsulfonyl)-2-[(1E)-prop-1-en-1-yl]aniline (Intermediate 60; 1.50 g; 6.84 mmol) and 10% Pd/C (196 mg) in MeOH (39 ml) was placed in a PARR reactor and treated with a pressure of 20 atm of hydrogen for 3 hours.

후처리

  1. customwas placed in a PARR reactor

출처 및 근거

ORD 기록
ord-a332f15c61344e31811bb892ece5d3f9
출처 데이터셋
uspto-grants-2012_09
특허 번호
US08273769B2

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