Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-bromo-N,N-dimethylbenzamide → HCID 58521976, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-bromo-N,N-dimethylbenzamide | HCID 3335826 | — |
| 반응물 | Tert-butyl(4-chloro-2-ethynylphenoxy)acetate | HCID 56594381 | — |
| 생성물 | HCID 58521976 | HCID 58521976 | — |
반응 단계
Following the general method as outlined in Intermediate 20, starting from (4-chloro-2-ethynyl-phenoxy)-acetic acid tert-butyl ester (Intermediate 3) and 3-bromo-N,N-dimethylbenzamide (Intermediate 180), the title compound was obtained as a brown sticky solid after purification by flash column chromatography (silica), eluting with cyclohexane containing increasing amounts of EtOAc.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08273769B2 |
| 출처 데이터셋 | uspto-grants-2012_09 |
| ORD ID | ord-7e477b5d4ae94c7f8f66875eaa2441cd |
| 출처 메모 | uspto-grants-2012_09 |