Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzylamine → N-(1,1-Dimethoxypropan-2-ylidene)-1-phenylmethanamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzylamine | HCID 7504 | — |
| 반응물 | Sulfuric acid magnesium salt (1:1) | HCID 24083 | — |
| 반응물 | Pyruvic aldehyde dimethyl acetal | HCID 80650 | — |
| 생성물 | N-(1,1-Dimethoxypropan-2-ylidene)-1-phenylmethanamine | HCID 71380533 | — |
반응 단계
12.9 mL 1,1-dimethoxyacetone was added to 10 mL benzylamine in 100 mL petrolether. Magnesiumsulfate was added and the reaction was stirred over night at RT. The mixture was filtered and evaporated to give 18.9 g of the desired product. (M+H)+: 209
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08642774B2 |
| 출처 데이터셋 | uspto-grants-2014_02 |
| ORD ID | ord-b3bc05dd952240c8a50ff875b993000c |
| 출처 메모 | uspto-grants-2014_02 |