Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-(Trifluoromethyl)phenol → 2-Hydroxy-5-trifluoromethylbenzaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-(Trifluoromethyl)phenol | HCID 67874 | — |
| 반응물 | Ethyl acetate hexane | HCID 21226206 | — |
| 생성물 | 2-Hydroxy-5-trifluoromethylbenzaldehyde | HCID 15500988 | 34% |
반응 단계
Following the general procedure and FCC purification with 30% ethyl acetate-hexane, 4-trifluoromethyl phenol (10.0 g, 61.7 mmol) gave 2-hydroxy-5-trifluoromethyl-benzaldehyde 27 (3.9 g, 34%) as a pink solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06855695B2 |
| 출처 데이터셋 | uspto-grants-2005_02 |
| ORD ID | ord-28e0930bac704493b0adc4c206e0474c |
| 출처 메모 | uspto-grants-2005_02 |