Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Fluorobenzohydrazide → 3,5-bis-(4-Fluoro-phenyl)-1H-(1,2,4)triazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Fluorobenzohydrazide | HCID 9972 | — |
| 반응물 | 4-Fluorobenzamidine | HCID 4295238 | — |
| 생성물 | 3,5-bis-(4-Fluoro-phenyl)-1H-(1,2,4)triazole | HCID 86686515 | 71.2% |
반응 단계
4 g 4-fluoro-benzamidine was mixed with 4.5 g 4-fluoro-benzoic acid hydrazide and the mixture was melted. Then the mixture was crystallized from ethyl acetate to yield 5.3 g of the desired compound. Rt: 1.55 min (method A), (M+H)+: 258
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08642774B2 |
| 출처 데이터셋 | uspto-grants-2014_02 |
| ORD ID | ord-a56a8ce5b21741e4a2db3ea3932a470a |
| 출처 메모 | uspto-grants-2014_02 |