N,N-dimethyl-N'-t-butyloxycarbonyl-N'-(2-methoxy-5-nitrophenyl)ethylenediamine → N,N-Dimethyl-N'-t-butyloxycarbonyl-N'-(5-amino-2-methoxyphenyl)ethylenediamine
반응식
[CH3:1][N:2]([CH3:24])[CH2:3][CH2:4][N:5]([C:17]([O:19][C:20]([CH3:23])([CH3:22])[CH3:21])=[O:18])[C:6]1[CH:11]=[C:10]([N+:12]([O-])=O)[CH:9]=[CH:8][C:7]=1[O:15][CH3:16].CC1C=C(C2OC(C)=NN=2)C=CC=1C1C=CC(C(O)=O)=CC=1>>[CH3:24][N:2]([CH3:1])[CH2:3][CH2:4][N:5]([C:17]([O:19][C:20]([CH3:22])([CH3:21])[CH3:23])=[O:18])[C:6]1[CH:11]=[C:10]([NH2:12])[CH:9]=[CH:8][C:7]=1[O:15][CH3:16]참가 물질
3
실험 절차
The title compound was prepared from N,N-dimethyl-N'-t-butyloxycarbonyl-N'-(2-methoxy-5-nitrophenyl)ethylenediamine (D20, 0.50 g, 0.0015 mol) using the method of Description 2 (0.37 g, 80%).
출처 및 근거
- ORD 기록
- ord-33f5b41b4b82410ca36f2129b5c6c9b8
- 출처 데이터셋
- uspto-grants-1998_09