4-Carboxyphenylboronic Acid → HCID 18980090, 화합물

반응식

Br[C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH:12]=[N:11][CH:10]=[N:9]2)=[CH:4][C:3]=1[CH3:13].B([C:17]1[CH:25]=[CH:24][C:20]([C:21]([OH:23])=[O:22])=[CH:19][CH:18]=1)(O)O>>[CH3:13][C:3]1[CH:4]=[C:5]([N:8]2[CH:12]=[N:11][CH:10]=[N:9]2)[CH:6]=[CH:7][C:2]=1[C:17]1[CH:25]=[CH:24][C:20]([C:21]([OH:23])=[O:22])=[CH:19][CH:18]=1

참가 물질

반응물 2

HCID 3121834-Carboxyphenylboronic Acid

HCID 189801161-(4-Bromo-3-methylphenyl)-1,2,4-triazole

생성물 1

HCID 18980090HCID 18980090, 화합물수율 63.9%

실험 절차

The title compound (0.15 g) was prepared from 1-(4-bromo-3-methylphenyl)-1,2,4-triazole (D63, 0.2 g) and 4-boronobenzoic acid (0.14 g) as described in Description 15.

출처 및 근거

ORD 기록: ord-6a7d17549ef44441ab544d0834f6d44b
출처 데이터셋: uspto-grants-1998_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05801170

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