Oxalyl chloride → 2,6-Di(propan-2-yl)benzoyl chloride
반응식
[CH:1]([C:4]1[CH:12]=[CH:11][CH:10]=[C:9]([CH:13]([CH3:15])[CH3:14])[C:5]=1[C:6](O)=[O:7])([CH3:3])[CH3:2].C(Cl)(=O)C([Cl:19])=O>CN(C)C=O>[CH:1]([C:4]1[CH:12]=[CH:11][CH:10]=[C:9]([CH:13]([CH3:15])[CH3:14])[C:5]=1[C:6]([Cl:19])=[O:7])([CH3:3])[CH3:2]참가 물질
4
실험 절차
A mixture of 2,6-diisopropylbenzoic acid (12.8 g, 0.062 mol), oxalyl chloride (25 mL), and dimethylformamide (2 drops) was stirred overnight at room temperature. The volatiles were removed on the rotary evaporator and the residue dried to yield an orange oil, 12.65 g, 90.9%.
후처리
- customThe volatiles were removed on the rotary evaporator
- customthe residue dried
- customto yield an orange oil, 12.65 g, 90.9%
출처 및 근거
- ORD 기록
- ord-b0fb921268f647aa8967e6289c301e33
- 출처 데이터셋
- uspto-grants-1998_09
- 특허 번호
- US05807846
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