참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | (R)-N5-[amino(nitroimino)methyl]-N-[(4-hydroxyphenyl)methyl)-ornithinamide | HCID 136381090 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | HCID 136381103 | HCID 136381103 | — |
반응 단계
0.3 g (0.925 mMol) of (R)-N5 -[amino(nitroimino)methyl]-N-[(4-hydroxyphenyl)methyl]-ornithinamide were dissolved in 3 ml of glacial acetic acid and after the addition of 3 ml (0.032 Mol) of acetic anhydride the mixture was heated to a reaction temperature of 50° C. for 30 minutes. The product remaining after the volatile components had evaporated off was further processed without purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05807875 |
|---|
| 출처 데이터셋 | uspto-grants-1998_09 |
|---|
| ORD ID | ord-31ea9a0506fa40a8941c09e0e2b196c5 |
|---|
| 출처 메모 | uspto-grants-1998_09 |
|---|
