Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → 4-[3-(2-Benzyloxyphenyl)propyl]benzene isocyanate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | P,P-Diphenylphosphinic azide | HCID 199401 | — |
| 반응물 | 4-(3-(2-Benzyloxyphenyl)propyl]benzoic acid | HCID 18973764 | — |
| 용매 | 1,4-Dioxane | HCID 31275 | — |
| 생성물 | 4-[3-(2-Benzyloxyphenyl)propyl]benzene isocyanate | HCID 18973742 | — |
반응 단계
The solution of 4-[3-(2-benzyloxyphenyl)propyl]benzene isocyanate in dioxane was prepared by heating a mixture of 4-[3-(2-benzyloxyphenyl)propyl]benzoic acid (2.0 g), Et3N (1.61 ml) and DPPA (1.31 ml) in dioxane (20 ml) for 3 hours.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05811459 |
| 출처 데이터셋 | uspto-grants-1998_09 |
| ORD ID | ord-b83d6244966c4f20a0d16ffeccfa4409 |
| 출처 메모 | uspto-grants-1998_09 |