Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-(2-Benzothiazol-2-ylthio)aniline → 1-[4-(2-Benzothiazolylthio)phenyl]-3-(4-chloro-3-trifluoromethylphenyl)thiourea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-(2-Benzothiazol-2-ylthio)aniline | HCID 117610 | — |
| 반응물 | 1-Chloro-4-isothiocyanato-2-(trifluoromethyl)benzene | HCID 520026 | — |
| 생성물 | 1-[4-(2-Benzothiazolylthio)phenyl]-3-(4-chloro-3-trifluoromethylphenyl)thiourea | HCID 18971677 | — |
반응 단계
2-(4-Aminophenylthio)benzothiazole (10.0 mmoles, 2.6 g) and 4-chloro-3-trifluoromethylphenylisothiocyanate 10.0 mmoles, 2.4 g) were reacted according to procedure C to yield of the title compound, 1.5 g, 30%. Mass Spec (FD) 495. Calculated for C21H13ClF3 N3S3 : C, 50.85H, 2.64N, 8.47. Found: C, 51.02; H, 2.71; N, 8.31.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05814646 |
| 출처 데이터셋 | uspto-grants-1998_09 |
| ORD ID | ord-3dec1a035fb04497968cce9aaa1d4d2f |
| 출처 메모 | uspto-grants-1998_09 |